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data-v-643f30a7=""><div data-v-643f30a7=""><p><br/></p><p><i class="img-wrapper" style="padding-bottom: 75%;"><img src="https://img76.chem17.com/gxhpic_034a220fb1/6fd5d5abffebbb9ef420fb13100c8c03a3375839606e7c87db0f4582a5044232687c56b5d3593cc0.jpg" loading="lazy"/></i></p><i class="img-wrapper" style="padding-bottom: 75.07%;"><img src="https://img78.chem17.com/gxhpic_034a220fb1/6fd5d5abffebbb9ef420fb13100c8c034fb1d6183676ca18659517266f8f40d4af4b600d6d4ebaf6.jpg" loading="lazy"/></i><i class="br"><br/></i><p>1．二氧化碳電極的主要參數及性能</p><p>1. 二氧化碳電極正常工作條件;</p><p>(1)空氣溫度:5-40℃</p><p>(2)相對濕度:≤85%</p><p>(3)被測液溫度: 5-60℃</p><p>(4)測量范圍:4.4 – 1760 ppm(mg/L)( 或1× 10-4- 4 × 10-2mol/L)</p><p>二氧化碳電極的級差≥理論值的90%</p><p>二氧化碳電極的內阻在25℃時(shí)300MΩ</p><p>二氧化碳電極的90%響應時(shí)間≤2分鐘（在880 ppm濃度溶液中,溶液溫度為25±2℃）</p><p>2．二氧化碳電極的結構，組裝及使用</p><p>電極頭次使用前應當擰開(kāi)電極后帽抽出玻璃內芯，在電極套管內加注內電解液(約1毫升)，然后再插入電極芯，旋上電極后帽，標定后測量使用。如果電極膜漏了，則要更換上備用電極膜頭。備用電極膜頭更換如下；先把電極后帽擰開(kāi)，抽出電極芯。然后擰下電極膜頭，旋上新的電極膜頭，用去離子水沖洗電極芯和電極套管三次，在電極套管內加注內電解液(約1毫升)，然后再插入電極芯，旋上電極后帽，標定后測量使用。</p><p>3. 二氧化碳電極的清洗</p><p>測試前,如果電極內部二氧化碳平衡濃度比待測樣二氧化碳濃度高,應當把二氧化碳電極響應清洗至待測樣濃度以下。如下；用柔軟的吸水紙輕輕吸干上次測定時(shí)電極頭部殘留的液滴,然后用去純凈水將電極頭部沖洗一下, 再用柔軟的吸水紙吸干表面水份，后在電極傾斜45度情況下(以利于驅除電極頭部氣泡)把電極插入盛有純凈水的三角瓶中，置于磁力攪拌器上在中速攪拌狀態(tài)下進(jìn)行清洗一直清洗到儀器上毫伏讀數值低于待測樣的響應毫伏值即可。如果要深度清洗，可以多換幾次清洗液,或者用電極深度清洗溶液在攪拌狀態(tài)下進(jìn)行清洗,以加快清洗速度。如果電極測前內部二氧化碳平衡濃度低于待測樣二氧化碳濃度，可不必清洗,或不必深度清洗。如果待測樣二氧化碳濃度較低，一定要深度清洗，這樣測量時(shí)才會(huì )有較快的響應和較準確的測量結果。清洗完畢的二氧化碳電極要浸在純凈水中備用或立即投入測量使用。</p><p>如果清洗時(shí)響應毫伏值不降反升或標定時(shí)響應毫伏值總是增大穩定不了,說(shuō)明膜有滲漏,應當</p><i class="br"><br/></i><i class="img-wrapper" style="padding-bottom: 141.33%;"></i><i class="br"><br/></i><i class="img-wrapper" style="padding-bottom: 141.33%;"></i><p 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